KnE Engineering | XIX International scientific-technical conference “The Ural school-seminar of metal scientists-young researchers” | pages: 158–162

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1. Intorduction

Friction stir processing with a rotating tool (FSP) is based on controlling intensive localized plastic deformation and high-speed thermal effect. FSP is applied for processing alloys containing aluminum, magnesium, copper, steels, etc. To control the FSP process the following variables are distinguished: tool rotating speed, feed and axial force [1. FSP normally employs a tool with a shoulder and a tip because of which various defects are likely to occur in the surface layer. To avoid internal defects tools with no tip but with a flat end face and a chamfer [3] are used. A kinematic diagramme illustrating FSP is presented in Figure 1.

fig-1.jpg
Figure 1
Kinematic diagramme of friction stir processing.

The paper [4] gives results of researching into FSP for the case of processing AISI 420 steel. It was determined that hardening of the surface layer is achieved through forming a martensitic structure. Strengthening surface layers in chromium steels by FSP with a tool that has a flat end face under the conditions when the effect of stirring is reduced to a minimum can be done predominantly by thermal action, through air hardening.

In this particular case it is essential that the surface layer should be heated to a temperature(T n ) exceeding the critical point Ac 3 = 950 С and pearlite be transformed into austenite.

To attain optimal results of hardening AISI 420 steel it is necessary to establish the impact of FSP variables on the structure and properties of the surface layer.

The selected process variables are expected to ensure heating to reach the temperature T n> Ac 3 and an appropriate conditioning time t cond at this temperature to transfer the friction heat to the surface layer. At the same time, overheating of the material must be avoided as in this case austenite grains will significantly grow in size which is likely to adversely affect strength, hardness and other mechanical properties.

Thus, proper process modes should be selected so that the α γ transformation could be ensured avoiding austenite grain growth. Analyzing a correlation between process variables and thermal parameters has made it possible to present it as a diagramme of hardening control (fig. 2).

fig-2.jpg
Figure 2
Diagramme showing hardening control.

2. Experimental Setup

The friction stir processing was conducted on a MA-600/Okuma milling machine centre making use of 100-mm diameter samples fabricated from AISI 420 steel, the original hardness being 187 HB while the microhardness after milling was 220-230 HV 0,05 . FSP was done with a Iskar tungsten carbide based hard-alloy tool with a flat end face end; the diameter of its body was 9 mm and its chamfer - 0,5x45 . The process variables are shown in table 1.

Table 1

The process variables.


№ exp. F n ,[N] f, [mm/min] n, [rev/min]
1 2500 100 3000
2 2500 150 3500
3 2500 200 4000
4 3000 100 3500
5 3000 150 4000
6 3000 200 3000
7 3500 100 4000
8 3500 150 3000
9 3500 200 3500

3. Results and Discussions

Metallographic samples were prepared to measure the microhardness of the surface layer at various depths after FSP. The plane lay at a 19 -degree angle in reference to the treated surface. Microhardness measurements were made along the central axis of each track by Vickers hardness test making use of a Leica VMHT microhardness tester with a 50 gf load applied on the indentor. HV 0,05 microhardness was measured along the depth with 10 µm incremental steps to the depth of 50 µm, with a 20 µm incremental step to the depth of 50 µm, a 50 µm step to the depth of 900 µm and a 100 µm step until the parent matrix was reached. 5 measurements were made at each depth.

fig-3.jpg
Figure 3
Changing of microhardness in depth.

The microhardness tests (fig. 3) showed that the deepest hardened layer of approximately 1,7 mm was obtained in sample №4 treated at F n =3000 N: f= 100 mm/min: n=3500 rev/min; and №7 produced at F n =3500 N: f= 100mm/min; n=4000 rev/min. Both modes have the slowest feed. This indicates that the feed is an important factor affecting not only the hardness but also the depth of the hardened layer. One more criterion of hardening the surface layer may be its thickness with a microhardness of 600 HV0, 05. The best treatment mode according to this criterion was used in experiment №4 when the thickness of the layer with a microhardness of 600 HV0, 05 was approximately 0,75 mm. Studying the microstructure of the working zone was done on an OLYMPUS optical microscope using SIAMS-700 software and x50 and x500 magnification. A post-FSP mictrostructural analysis of the surface layer showed the formation of a zone of parabolic shape where the modified mictrostructure is observed (fig. 4). In this zone 3 areas emerge. In area 1 next to the treated surface, a martensitic structure with dispersed inclusions of carbides can be seen (fig 5, a). A microstructural analysis at a depth of 500 µm showed that the formation of a homogeneous martensitic structure is ensured only if the feed is 100 mm/min (fig. 5, b). At 1000 µm from the surface and 100 mm/min feed a composite martensitic-perlite structure with dispersed inclusions of carbides is formed (fig. 5, c). When the feed values are 150 and 200 mm/min, at a depth of 1000 µm no changes in the microstructure occur

fig-4.jpg
Figure 4
Microstructure of the surface layer at x50 magnification of experiment №4.
fig-5.jpg
Figure 5
Microstucture of a hardened layer at x500 magnification F н = 3000 N; f = 100 mm/min; n = 3500rev/min.

4. Conclusions

Comparing the microstructure measurements and the microstructural analysis of the modified and original materials together with the temperature changes in the FSP at various combinations of process variables gives grounds to draw the conclusion that the conditioning time at maximum temperature has a decisive influence on the thickness of the hardened layer.

References

1 

Mishra R.S., Ma Z.Y. Friction stir welding and processing/ R.S. Mishra, Z.Y. Ma // Materials Science and Engineering R 50 (2005) 1–78; doi:10.1016/j.mser.2005.07.001.

2 

Rai R. Review: friction stir welding tools/ R. Rai, A. De, H. K. D. H. Bhadeshia and T. DebRoy// Science and Technology of Welding and Joining, 2011.

3 

Zhang Y. N. Review of tools for friction stir welding and processing / Y. N. Zhang, X. Cao, S. Larose and P. Wanjara // Canadian Metallurgical Quarterly, 2012.

4 

Dodds S. Tribological enhancement of AISI 420 martensitic stainless steel through friction-stir processing/ S. Dodds, A.H.Jones, S.Cater // Wear, 2013; dx.doi.org/10.1016/j.wear.2013.01.007i.

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